新丰中子核素~(185)Hf的研究Ⅱ.合成和鉴别中的快放射化学分离

    • 摘要: 介绍了在新丰中子核素 ̄(185)Hf合成和鉴别过程中快放射化学分离流程的研制和实验。用沉淀剂使Hf生成BaHfF_6沉淀而与大量的靶物质钨及其他伴随产物分离,所得沉淀制源后,测其γ放射性。整个流程典型分离时间约6-7min,化学回收率约53%,去污系数完全满足新丰中子核素 ̄(185)Hf的合成和鉴别的要求。

       

      Abstract: STUDY OF NEW NEUTRON-RICH NUCLIDE ~(185)Hf Ⅱ.THE RAPID-CHEMICAL SEPARATION STUDY ON THE SYNTHESIS AND IDENTIFICATIONZNANG TIANMEI;CHEN JIGREN;YUAN SHUANGGUI;PAN QIANGYAN;ZHANG XUEQIAN;XU SHUWEI(Institute of Modern Physics,Chinese Academy of Sciences,Lanzhou 730000)(Department of Modern Physics,Lanzhou University,Lanzhou 730000)ABSTRACT The development and experiment of rapid-chemical separation procedure on the synthesisand identification of new neutron-rich nuclide ~(185)Hf are reported.Hafnium is precipitated in theform of BaHfF_6 ,then is seperated from tangsten,tantalum and other reaction products. The pre-cipitate is used as a source to be measured to obtain its γ-ray spectroscopy. The typical separation time of this procedure is about 6-7min and the chemical efficiency is53%. Contamination activities of Ta and W have been reduced to 5%and 8%,respectively. Key words New neutron nuclide~(185)Hf Precipitation method BaHfF_6

       

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