Abstract: RAPID RADIOCHEMICAL ANALYSIS OF ~(114)Pd FROM THE PRODUCTS OF ~(252)Cf SPONTANEOUD FISSIONYU RUNLAN；CUI ANZHI；LI XUELIANG；GUO JINGRU；YAN SHUHENG；TANG PEUIJIA；LIU DAMING（China Institute of Atomic Energy，P，O.Box 275（26），Beijing 102413）ABSTRACT A manual rapid procedure has been developed to analyse ~(114)Pd from prducts of ~(252)Cf sponta-neous fission. The main steps of the procedure are extraction and precipitation of Pd（DMG）_2complex.It takes 5． 5 to 6 min to complete the separation procedure. The chemical recovery is inthe range of 30％-60％and the precision in relative standard deviation for single analysis is3．9％.Key words ~(114)Pd Rapid radiochemical analysis ~(252)Cf