PRECISE DETERMINATION OF TRACE ACTINIDES Ⅳ, FLUORESCENCE COMPLEXOMETRIC TITRA-TION OF A FEW MICROGRAMS OF NEPTUNIUM AND AMERICIUM
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Graphical Abstract
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Abstract
The procedure of unusual fluorescence complexometric titration has been applied to the determination of a few micrograms of Np and Am. Np (Ⅴ) is pre-reduced to Np (Ⅳ) by NH2OH·HCl. The relative standard deviation for the determination of 5μg Np is less than ±0.5%; and that for 2μg Np or Am is less than±1%.
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