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TAN Shu-ping, MA Gui-lan. Determination of Solubility of TBOPDA in the Different Concentration of HNO3 by Gas Chromatography[J]. Journal of Nuclear and Radiochemistry, 2010, 32(3): 189-192.
Citation: TAN Shu-ping, MA Gui-lan. Determination of Solubility of TBOPDA in the Different Concentration of HNO3 by Gas Chromatography[J]. Journal of Nuclear and Radiochemistry, 2010, 32(3): 189-192.
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Determination of Solubility of TBOPDA in the Different Concentration of HNO3 by Gas Chromatography

  • China Institute of Atomic Energy, P.O. Box 275(88), Beijing 102413, China

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  • Received Date: December 31, 1899
  • Revised Date: December 31, 1899
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  • In this paper, a gas chromatograhic assay for TBOPDA with flame ionization detector (FID) and Porapak-Qs column was used. First, the equal volume of 0.2 mol/L TBOPDA /40% octanol-OK and HNO3 were shaked for 40 min, then TBOPDA in the liquid phase with methylbenzene was extracted, and last organic phase with gas chromatography was analyzed. Solubility of TBOPDA in the concentration of 1, 2, 3 mol/L HNO3 is respectively 0.702, 0.723, 0.735 g/L.
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    • References (3)
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    叶国安.Purex流程中镎在1A槽的走向控制和新型萃取剂酰胺荚醚的萃取热力学及应用研究[D].北京：中国原子能研究科学院，2002.
    [2]
    Abaroudi K, Trabelsi F, Recasens F. Quasi-Static Measurement of Equilibrium Solubilities in SC Fluids: A Mass Transfer Criterion[J]. Fluid Phase Equilibria, 2000, 169: 177.
    [3]
    Urszuka D, Warren C M. Solubility of Sulfolane in Selected Organic Solvents[J]. J Chem Eng Data, 1996, 41: 261.
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